An oscillatory ball mill (Mixer Mill MM301 Retsch Co. Germany) was used for cryo milling as follows 1 g of indomethacin was placed into a 25 mL milling jar and milled with two 12 mm balls for 120 minutes. The jars were immersed in liquid nitrogen for 3 min before milling and repeatedly for 3 min at 15 min intervals. Get Price
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