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The precursor is then ball-milled under argon with the corresponding amount of antimony (Alfa Aesar, < 6 mm pellet size, 5 N purity), with either PBM for 12 h (Retsch PM 400, 250 rotations per minute (RPM), stop and reversal of rotation every 10 min, stainless steel jar and balls, powder to ball ratio PBR 10:3, dry) or HEBM for 5 h (SPEX 8000 D ...
The particles formed small spheres or balls with a range of diameter about 0.5–3 mm. They presented a weak compaction so that the original consistence of the particles could be restored with a soft compression. The color of the product was close to the 1 red of Cu 2 O. In order to corroborate the composition of the powdered product, it was ...
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